Sem/eds analysis laboratories with Microvisionlabs.com? The unique properties of birefringence allow for the differentiation of fibers, minerals, ceramics, and other biological materials. Particles can therefore be identified and comparatively quantified, resulting in the characterization of the components of a sample. Complimentary optical techniques such as Nomarski/DIC, bright field and dark field imaging add to the amount of information our Optical Analysts can obtain from your samples. Additionally we have a range of light sources and filters to outfit our stereo microscopes for fluorescent microscopy.
Analysis and Results: The submitted bottle was examined for signs of interior distress, and the water from the bottle was removed and maintained. Some of the suspended particulate was filtered and examined non-destructively by light microscopy first, to characterize the material. A low magnification stereo microscope image of the filtered white particulate is shown in the image above. From this image, biological tissues were ruled out, and the material was observed to be crystalline. Polarized light microscopy (PLM) was used to analyze the sample next. From this examination, the material showed birefringence as shown in the PLM image on the right. The PLM Image Stereo Microscope image suspect material showed optical properties and morphology dissimilar to common carbonates and sulfates. It was determined to be a birefringent crystalline material, but it could not be identified using only PLM methods. Therefore, analysis using scanning electron microscopy with energy dispersive x-ray spectroscopy (SEM-EDS) would have to be performed to obtain further information about the suspect material.
Scanning electron microscopy with energy dispersive xray spectroscopy (SEM-EDS) was used to identify the particles. The SEM showed an elevated concentration of iron and iron oxide in the impacted areas. The backscatter electron (BSE) image which correlates brightness in the image with atomic density, highlighted the iron particles that were embedded in the tile and the EDS spectrum confirms the PLM Image chemical composition of these higher density particles.
Do you give lab tours? Yes, we routinely give lab tours to our clients and potential clients. Please call and we would be happy to schedule a tour for you and your co-workers. Do you have other locations around the country? We do work for companies all across the United States, with one laboratory which is located in Chelmsford, Massachusetts. Did MicroVision Labs ever operate under a different company name? No, we have always been MicroVision Laboratories, Inc. Our founder, John Knowles, used to work for another laboratory that underwent several name changes (Eastern Analytical Laboratories, Industrial Environmental Analysts, American Environmental Network, Severn Trent Laboratories, and EMLab P&K Billeria) and was located nearby in Billerica. When that laboratory was closed in 2008, John hired a few of the remaining analysts and acquired its equipment, client list and phone number. Find even more details at https://microvisionlabs.com/service/sem/.
The client was contacted with the results, and was curious as to what the source of these particles might be. After consulting with the office manager, it was determined that some pieces of furniture present had relatively significant amounts of direct water exposure, and were subsequently dried a number of times during remittance construction. Inspection of these pieces of furniture showed that they had high density, close packed foam cushions of a type similar to the particles observed in the surrounding area, which had been broken down by the repeated wet/dry cycle.
?We partner with companies in all phases of product development and sales, including R&D, manufacturing, QC, advertising and failure analysis. Our laboratory offers a highly-trained and experienced staff utilizing a powerful set of analytical tools (SEM with EDS and backscatter detectors, Bruker X-Flash elemental mapping, X-Ray imaging, Micro-FTIR spectroscopy, Micro-XRF, light microscopy, cross sectioning/precision polishing and microhardness testing). See more info on https://microvisionlabs.com/.